超声波辅助提取五倍子单宁酸的响应面优化实验

›› 2012, Vol. 46 ›› Issue (6): 12-16.

• 研究报告 • Previous Articles Next Articles

Optimization of Ultrasonic-assisted Extraction of Tannic Acid from Chinese Gallnut Using Response Surface Method

ZHANG Zong-he^1,2, MIN Fan-qin², QIN Qing^1,2, XU Hao^1,2, LI Wen-jun², WANG Cheng-zhang^1,2

1. Nanjing Longyuan Natural Polyphenols Synthesis Factory, Nanjing 210032, China;2. Institute of Chemical Industry of Forestry Products, CAF; National Engineering Lab.for Biomass Chemical Utilization; Key and Open Lab.of Forest Chemical Engineering, SFA; Key Lab.of Biomass Energy and Material, Jiangsu Province, Nanjing 210042, China

Received:2012-09-28 Revised:1900-01-01 Online:2012-11-30 Published:2012-11-30

Abstract

Abstract: The ultrasonic-assisted extraction of tannic acid from Chinese gallnut with water as extraction agent were determined on the basis of single factor experiment using response surface method (RSM). According to central composite (Box-Behnken) design principle, the effect of three independent variables on the yield of tannic acid, namely liquid to solid ratio, ultrasonic extraction time, and ultrasonic power was investigated. The results showed the optimum ultrasonic-assisted extraction conditions were: 5 g of Chinese gallnut powder, liquid to solid ratio 38:1 (mL:g), ultrasonic extraction time 32 min, ultrasonic power 250 W. Under the optimum conditions, the extraction yield of tannic acid was 66.0%.

Key words: Chinese gallnut, tannic acid, response surface method, exaction, ultrasonic

CLC Number:

TQ35

ZHANG Zong-he;MIN Fan-qin;QIN Qing;XU Hao;LI Wen-jun;WANG Cheng-zhang;. Optimization of Ultrasonic-assisted Extraction of Tannic Acid from Chinese Gallnut Using Response Surface Method[J]. , 2012, 46(6): 12-16.

[1]	Jie REN,Li WAN,Nanwei CHEN,Fan YANG,Shuiyu SUN,Suizhou REN. Preparation and Characterization of Activated Carbon from Coffee Grounds and Its Adsorption Mechanism for Cr(Ⅵ) [J]. Biomass Chemical Engineering, 2020, 54(4): 1-8.
[2]	Qiqi DAI,Xiaocui WEI,Hongbiao TANG,Jin LI,Jinjing WANG. Optimization of Microwave Assisted Pyrolysis of Coconut Clothes by Response Surface Method and Analysis of Liquid Product Composition [J]. Biomass Chemical Engineering, 2020, 54(4): 42-48.
[3]	Zhiwen QI,Chengzhang WANG,Jianxin JIANG. Isolation and Physical-chemical Data Testing of Levopimaric Acid [J]. Biomass Chemical Engineering, 2019, 53(6): 45-50.
[4]	Cunxin XIE,Yongjun DENG,Jian JIAO,Hongbin LI,Ting WU,Guigan FANG. Analysis of Ultrasonic Assisted Wood-chip Impregnation at Atmospheric Pressure and Bleaching [J]. Biomass Chemical Engineering, 2019, 53(5): 34-38.
[5]	WANG Yonggui, REN Shuzhi, GENG Qingbao, ZHANG Weigang, GE Xiutao. Optimization of 5-Hydroxymethylfurfural Preparation from Hydrolysis of Maltose Dehydration by Response Surface Methodology [J]. bce, 2018, 52(6): 57-61.
[6]	QIAN Jingru, LI Weiyu, YI Zhengming. Optimization of Preparing Conditions of Oil in Water Natural Rosin Emulsion by Response Surface Method [J]. bce, 2018, 52(2): 12-17.
[7]	GUO Xiangqin, CAI Na, YANG Shanbin, ZHOU Shiyang, CHEN Yixin, KE Daoyao. Preliminary Research on Ultrasonic Assisted Extraction Technology of Polysaccharides in Ginkgo biloba Leaves [J]. bce, 2017, 51(6): 43-47.
[8]	ZHAO Houkuan, WANG Peng, XIE Xingpeng, YE Zhezi, XIE Yimin. Inhibition of Free Formaldehyde in Synthesis of Urea-formaldehyde Resin [J]. bce, 2017, 51(1): 20-26.
[9]	LI Yan-fang, GAO Cai-xia, GAO Yang, HAN Xiang-en. Ultrasonic-assisted Extraction and Antioxidant Activity of Polyphenols from Koelreuteria paniculata Laxm. Leaves [J]. bce, 2016, 50(3): 27-34.
[10]	WANG Yan-yun, YANG Jing. Influence of Alkaline-Fenton Pretreatment on the Enzymatic Hydrolysis Yield of Yunnan Bamboo [J]. bce, 2015, 49(5): 17-22.
[11]	ZHANG Wei, ZHANG Qi, RUAN Xin-yi, WANG Xin-ze, KONG Hai-nan, LIN Yan. Optimization of Enzymatic Hydrolysis of Wheat Straw by Using Response Surface Methodology [J]. bce, 2015, 49(2): 39-46,52.
[12]	TAO Ran, WANG Cheng-zhang, ZHANG Yu-si, YE Jian-zhong, ZHOU Hao, CHEN Hong-xia. Preparation of Polyprenols Nanoemulsion from Ginkgo biloba L. Leaves Polyprenols [J]. bce, 2015, 49(1): 7-12.
[13]	ZHANG Yu-si, WANG Cheng-zhang, SHU A-qing, YE Jian-zhong. Optimization of Ultrasonic-assisted Extraction of Polyphenol from Litsea Coreana using Response Surface Methodology [J]. bce, 2014, 48(5): 19-23.
[14]	JIANG Ping, HU Hai-ke, DU Qing-lin. Optimization of Synthesis of 2,3,4-Trihydroxybenzoic Acid with Water by Response Surface Method [J]. bce, 2014, 48(3): 36-39.
[15]	TAN Fei, LIN Yong-mei, WANG Su-mei, ZHENG Zhang-wei, HUANG Biao. Optimization of Lignin Extraction from Black Liquor by Phosphoric Acid Using Response Surface Methodology [J]. bce, 2014, 48(2): 8-12.

Optimization of Ultrasonic-assisted Extraction of Tannic Acid from Chinese Gallnut Using Response Surface Method

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments