竹焦油-糠醛热固性树脂的制备及性能表征

›› 2012, Vol. 46 ›› Issue (4): 17-21.

• 研究报告 • Previous Articles Next Articles

Preparation and Characterization of the Bamboo Tar-furfural Thermosetting Resin

WANG Jia-xun¹, YUN Jun-xian¹, CHEN Shun-wei², SHEN Shao-chuan¹, ZHUANG Xiao-wei², YAO Ke-jian¹, GAO Yun-ling¹

1. Zhejiang University of Technology, College of Chemical Engineering & Materials Science, Hangzhou 310014, China;2. Zhejiang Forestry Academy, Zhejiang Provincial Key Laboratory of Biological and Chemical Utilization of Forest Resources, Hangzhou 310023, China

Received:2012-02-13 Revised:1900-01-01 Online:2012-07-30 Published:2012-07-30

Abstract

Abstract: Bamboo-tar furfural thermosetting resin (BTFF) was synthesized by bamboo tar and furfural under catalysis of alkaline. The solid content and the viscosity of the BTFF increased, with the increase of reaction temperature and time, while the residue furfural contents reduced. The pH of the prepared BTFF was 9-10, and the density was 1.20-1.30 g/mL. The properties of BTFF were analyzed by Fourier transform infrared spectroscopy (FT-IR) and differential scanning calorimetry (DSC). The results showed that the chemical structures of BTFF were similar to those of the phenol-furfural resin (PFF). By DSC, the BTFF was cured at a low temperature (150℃) which was close to that of PFF.

Key words: bamboo tar, furfural, thermosetting, property, resin

CLC Number:

TQ351

WANG Jia-xun;YUN Jun-xian;CHEN Shun-wei;SHEN Shao-chuan;ZHUANG Xiao-wei;YAO Ke-jian;GAO Yun-ling. Preparation and Characterization of the Bamboo Tar-furfural Thermosetting Resin[J]. , 2012, 46(4): 17-21.

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Preparation and Characterization of the Bamboo Tar-furfural Thermosetting Resin

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