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›› 2007, Vol. 41 ›› Issue (4): 13-16.

• 研究报告 • Previous Articles     Next Articles

Study on Preparation of Levulinic Acid by Acid Hydrolysis of Rice Straw

LIU Kai, FANG Gui-zhen, MA Yan-li, ZHAO Ying-li   

  1. Key Laboratory of Bio-based Material Science and Technology, Northeast Forestry University, Ministry of Education, Harbin 150040, China
  • Received:2007-02-05 Revised:1900-01-01 Online:2007-07-30 Published:2007-07-30

Abstract: Levulinic acid was prepared by the method of high-pressure acid hydrolysis of rice straw. The purity of levulinic acid was determined by gas chromatography. The influences of the reaction temperature, reaction time, solid-liquid ratio and acid concentration on the yield of levulinic acid were investigated. The single factor experimental results showed that when the temperature was 170℃, the solid- liquid ratio was 1:10 and the acid concentration was 5% by mass, the yield of levulinic acid was 24.35%. At this optimal hydrolysis condition, no cellulose or pentosan was detected in the hydrolyzed residue.

Key words: levulinic acid, rice straw, acid hydrolysis

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