Biomass Chemical Engineering ›› 2022, Vol. 56 ›› Issue (1): 57-66.doi: 10.3969/j.issn.1673-5854.2022.01.008
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Meijuan ZHONG, Xing′e LIU, Lili SHANG, Genlin TIAN, Shumin YANG, Jianfeng MA()
Received:
2020-09-14
Online:
2022-01-30
Published:
2022-01-18
Contact:
Jianfeng MA
E-mail:Majf@icbr.ac.cn
CLC Number:
Meijuan ZHONG, Xing′e LIU, Lili SHANG, Genlin TIAN, Shumin YANG, Jianfeng MA. Research Advance on Adjustment of Pore Structure of Plant-based Activated Carbon[J]. Biomass Chemical Engineering, 2022, 56(1): 57-66.
Table 1
Comparison of characteristics of cellulose, hemicelluloses and lignin after carbonization and activation"
组分 components | 热解温度/℃ pyrolysis temperature | 炭得率 char yield | 炭化后孔隙特征 pore characteristics after carbonization | 活化后孔隙特征 pore characteristics after activation |
纤维素 cellulose | 315-400 | 聚合度高于半纤维素,炭得率居于木质素和半纤维素之间 the degree of polymerization is higher than that of hemicellulose, and the carbon yield is between that of lignin and hemicellulose | 微孔为主,比表面积最大 the pores are mainly micropores with the largest specific surface area | 具有微介孔结构,比表面积最大 it has microporous and mesoporous structure with the largest specific surface area |
半纤维素 hemicelluloses | 220-315 | 含有大量的羟基且稳定性较差,炭得率最低 the carbon yield is the lowest because of lots of hydroxyl groups and poor stability | 微孔为主,比表面积居于木质素和纤维素之间 the pores are mainly micropores, and the specific surface area is between that of lignin and cellulose | 具有微介孔结构,比表面积最小 it has microporous and mesoporous structure with the smallest specific surface area |
木质素 lignin | 160-900 | 含有大量芳香结构,稳定性最高,炭得率最高 the char yield is the highest because of lots of aromatic structure | 微孔为主,比表面积最小 the pores are mainly micropores, and the specific surface area is the smallest | 具有微介孔结构,比表面积居于纤维素和半纤维素之间 it has microporous and mesoporous structure and the specific surface area is between that of cellulose and hemicellulose |
Table 2
Characteristics of the pore of activated carbon prepared by different activation methods"
活化方法 activation methods | 原料 materials | 总比表面积/(m2·g-1) total specific surface area | 微孔比表面积/(m2·g-1) specific surface area of micropore | 总孔容/(cm3·g-1) total pore volume | 微孔孔容/(cm3·g) micropore volume | 平均孔径/nm mean diameter | 参考文献 ref. |
CO2活化 CO2 activation | 可可豆荚壳 cocoa pod husk | 351.8-1329.8 | 305-1073.5 | 0.187-0.707 | 0.156-0.551 | 2.09-2.17 | [ |
稻壳rice husk | 175.2-215.8 | — | 0.1155-0.1296 | 0.0625-0.0698 | 2.402-2.6370 | [ | |
蓝焦blue coke | 75.5-636.91 | 48.22-457.4 | 0.059-0.363 | 0.029-0.201 | 1.89-3.1199 | [ | |
橡胶木屑 rubber wood sawdust | 302-465 | — | 0.154-0.239 | 0.135-0.186 | — | [ | |
H2O活化 H2O activation | 茶叶渣waste tea | 995.07 | — | 0.678 | 0.678 | — | [ |
油菜籽粕 canola meal | 240-386 | — | — | — | 1.55-2.58 | [ | |
大麦秆barley straw | 530-552 | 500-540 | 0.2440-0.2994 | 0.2210-0.2304 | 1.843-2.235 | [ | |
KOH活化 KOH activation | 橄榄核olive pits | 1344-1815 | — | — | — | 0.7-1.38 | [ |
烟梗tobacco stems | 609-1437 | — | 0.240-1.007 | 0.126-0.771 | 0.58-1.52 | [ | |
稻壳rice husk | 778.36-1818.45 | — | 0.39-0.90 | 0.28-0.84 | 1.2-1.85 | [ | |
H3PO4活化 H3PO4 ctivation | 枣核date pits | 1040 | 221 | 1.089 | 0.084 | 3.18 | [ |
柳枝稷 kanlow switchgrass | 1372.93 | 137.05 | 1.45 | 0.1 | 3.42 | [ | |
芒草 public miscanthus | 999.06 | 284.51 | 1.04 | 0.12 | 4.15 | [ | |
竹子bamboo | 244.5-398.4 | — | 0.153-0.680 | — | 1.256-3.975 | [ | |
ZnCl2活化 ZnCl2 activation | 卷心菜 sewage sludge | 133.22 | — | 0.15 | 0.016 | 12.51 | [ |
纺织废黄麻 textile waste jute | 1224 | 662 | 0.66 | 0.26 | — | [ | |
FeCl3活化 FeCl3 activation | 编织废棉 waste cotton woven | 748 | 642 | 0.606 | 0.253 | — | [ |
橙皮orange peel | 1802.1 | 1680.2 | 0.8761 | 0.8681 | — | [ | |
枣核date pits | 780 | — | 0.573 | 0.468 | [ | ||
热解自活化 self-activation | 椰壳coconut shell | 1194 | — | 0.528 | 0.446 | — | [ |
红麻芯纤维 kenaf core fibers | 2296 | — | 1.876 | 0.513 | — | [ |
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