响应曲面法优化水包油型天然松香乳液的制备

doi:10.3969/j.issn.1673-5854.2018.02.003

Abstract

Abstract: Oil in water(O/W) natural rosin emulsion was prepared by the method of normal pressure phase inversion emulsification with natural rosin as raw material and ONIST APS-350 as emulsifter. The influences of emulsifier dosage, initial emulsification temperature, oil-water ratio(the mass ratio of rosin and water) and stirring speed on the particle size distribution of O/W natural rosin emulsion were investigated, and then the response surface method(RSM) was used to simulate and optimize the process parameters. The results showed that the optimum parameters were determined as follows:stirring speed 500 r/min, emulsifier dosage 9.95%, temperature 112℃, and oil-water ratio 10:31. Under these conditions, the average particle size of emulsion was 131.1nm, the emulsion was not stratified by centrifugal force and not stratified for 3 months. The results of TEM showed that the particles had core-shell structure, and the particle size was consistent with the experimental value.

Key words: natural rosin, aqueous emulsion, core shell structure, process optimization, response surface method

CLC Number:

TQ351.47

QIAN Jingru, LI Weiyu, YI Zhengming. Optimization of Preparing Conditions of Oil in Water Natural Rosin Emulsion by Response Surface Method[J]. bce, 2018, 52(2): 12-17.

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Optimization of Preparing Conditions of Oil in Water Natural Rosin Emulsion by Response Surface Method

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