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bce ›› 2016, Vol. 50 ›› Issue (4): 42-46.doi: 10.3969/j.issn.1673-5854.2016.04.008

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Purification of Polyphenols from Koelreuteria paniculata Laxm. Leaves by Macroporous Resin

LI Yan-fang1,2, GAO Cai-xia3, HAN Xiang-en1   

  1. 1. China University of Mining and Technology, School of Chemical Engineering and Technology, Xuzhou 221116, China;
    2. Xuzhou Products Quality Supervision and Inspection Center, Xuzhou 221000, China;
    3. Beijing Haiderun Pharmaceutical Co. Ltd, Beijing 101113, China
  • Received:2015-12-29 Online:2016-07-31 Published:2016-10-08

Abstract: The absorption and desorption behaviors of seven macroporous resins for polyphenols from Koelreuteria paniculata Laxm. were investigated. The 24h static adsorption capacity and desorption rate of AB-8 resin was 13.74mg/g and 98.35%, respectively. The static adsorption and desorption equilibrium time of AB-8 resin was both less than 3h. The optimum conditions of dynamic absorption and desorption by AB-8 were sample mass concentration 4g/L, sample pH value 6, and volume fraction of ethanol 60%, elution speed 1mL/min, respectively.Under these conditions, the adsorption rate was 88.21% and desorption rate was 89.91%.The purity of polyphenols from Koelreuteria paniculata Laxm. increased from 50.36% to 72.37% after purification using AB-8 resin and the recovery rate was 86.83%.

Key words: polyphenols of Koelreuteria paniculata Laxm. Leaves, purification, macroporous resin

CLC Number: